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流变 流变实验数据及处理选用的实验对象是PE含量为50%的模压的样品
一． AS实验数据
Data Series Information
Name:
PE50% KETIZU 1
Number of Intervals:
1
Application:
RHEOPLUS/32 V3.61 21005914-33024
Device:
MCR302 SN81054732; FW3.64; Slot(6,-1); Adj(44,0)d
Measuring Date/Time:
2014-11-27; 10:35 上午
Measuring System:
PP25-SN27510; [d=1 mm]
Accessories:
TU1=CTD450L+R+L-PP-SN81021826-0-17497206; BiO2=OMNICURE
Calculating Constants:
- Norm. Csr [min/s]:
1.307541
- Norm. Css [Pa/mNm]:
327.0391
- Start Delay Time [s]:
255.109
- Substance Density [rho]:
1,000
- Measurement Type:
1
- Axial Compliance [m/N]:
1.00E-06
- Position [m]:
1.00E-06
Interval:
1
Number of Data Points:
21
Time Setting:
21 Meas. Pts.
Measuring Profile:
0
Amplitude gamma = 0.01 ... 100 % log; |Slope| = 5 Pt. / dec
Angular Frequency omega = 10 rad/s
Meas. Pts.
Strain
Shear Stress
Storage Modulus
Loss Modulus
Damping Factor
Deflection Angle
Torque
Status
[%]
[Pa]
[Pa]
[Pa]
[1]
[mrad]
[μNm]
[]
1
0.01
1.47E+00
8.72E+03
1.18E+04
1.35
0.00801
4.49
DSO
2
0.0158
2.32E+00
8.70E+03
1.18E+04
1.35
0.0127
7.09
DSO
3
0.0251
3.69E+00
8.72E+03
1.18E+04
1.35
0.0201
11.3
DSO
4
0.0398
5.88E+00
8.78E+03
1.19E+04
1.35
0.0319
18
DSO
5
0.0631
9.34E+00
8.80E+03
1.19E+04
1.35
0.0505
28.6
DSO
6
0.1
1.48E+01
8.81E+03
1.19E+04
1.35
0.0801
45.3
DSO
7
0.158
2.36E+01
8.83E+03
1.20E+04
1.35
0.127
72
DSO
8
0.251
3.74E+01
8.85E+03
1.20E+04
1.35
0.201
114
DSO
9
0.398
5.94E+01
8.87E+03
1.20E+04
1.35
0.319
182
DSO
10
0.631
9.44E+01
8.90E+03
1.20E+04
1.35
0.505
289
DSO
11
1
1.50E+02
8.95E+03
1.21E+04
1.35
0.801
460
DSO
12
1.58
2.40E+02
9.00E+03
1.22E+04
1.35
1.27
733
DSO
13
2.51
3.82E+02
9.04E+03
1.22E+04
1.35
2.01
1,170
DSO
14
3.98
6.04E+02
9.02E+03
1.22E+04
1.35
3.19
1,850
DSO
15
6.31
9.59E+02
9.04E+03
1.22E+04
1.35
5.05
2,930
DSO
16
10
1.52E+03
9.02E+03
1.22E+04
1.35
8.01
4,640
DSO
17
15.8
2.40E+03
8.98E+03
1.22E+04
1.36
12.7
7,340
DSO
18
25.1
3.77E+03
8.86E+03
1.21E+04
1.37
20.1
11,500
DSO
19
39.8
5.88E+03
8.60E+03
1.20E+04
1.4
31.9
18,000
DSO
20
63.1
8.92E+03
8.05E+03
1.16E+04
1.44
50.5
27,300
DSO
21
100
1.28E+04
6.98E+03
1.08E+04
1.54
80.1
39,300
DSO
二．AS数据处理
三．FS实验数据
Data Series Information
Name:
PE50% KETIZU 1
Number of Intervals:
1
Application:
RHEOPLUS/32 V3.61 21005914-33024
Device:
MCR302 SN81054732; FW3.64; Slot(6,-1); Adj(44,0)d
Measuring Date/Time:
2014-11-27; 10:42 上午
Measuring System:
PP25-SN27510; [d=1 mm]
Accessories:
TU1=CTD450L+R+L-PP-SN81021826-0-17497206; BiO2=OMNICURE
Calculating Constants:
- Norm. Csr [min/s]:
1.307541
- Norm. Css [Pa/mNm]:
327.0391
- Start Delay Time [s]:
65.906
- Substance Density [rho]:
1,000
- Measurement Type:
1
- Axial Compliance [m/N]:
1.00E-06
- Position [m]:
1.00E-06
Interval:
1
Number of Data Points:
16
Time Setting:
16 Meas. Pts.
Measuring Profile:
#NAME?
Amplitude gamma = 1 %
Angular Frequency omega = 100 ... 0.1 rad/s log; |Slope| = 5 Pt. / dec
Meas. Pts.
Angular Frequency
Storage Modulus
Loss Modulus
Damping Factor
Complex Viscosity
Deflection Angle
Torque
Status
[1/s]
[Pa]
[Pa]
[1]
[Pa·s]
[mrad]
[μNm]
[]
1
100
3.68E+04
3.14E+04
0.853
4.84E+02
8.00E-01
1.48E+03
DSO
2
63.1
2.85E+04
2.68E+04
0.943
6.20E+02
7.95E-01
1.19E+03
DSO
3
39.8
2.21E+04
2.25E+04
1.02
7.91E+02
8.01E-01
9.63E+02
DSO
4
25.1
1.66E+04
1.85E+04
1.11
9.90E+02
8.01E-01
7.61E+02
DSO
5
15.8
1.23E+04
1.50E+04
1.22
1.22E+03
8.00E-01
5.91E+02
DSO
6
10
8.82E+03
1.19E+04
1.35
1.48E+03
8.01E-01
4.53E+02
DSO
7
6.31
6.22E+03
9.31E+03
1.5
1.77E+03
8.01E-01
3.42E+02
DSO
8
3.98
4.28E+03
7.16E+03
1.67
2.10E+03
8.01E-01
2.55E+02
DSO
9
2.51
2.89E+03
5.41E+03
1.87
2.44E+03
8.01E-01
1.87E+02
DSO
10
1.58
1.89E+03
4.01E+03
2.12
2.80E+03
8.01E-01
1.35E+02
DSO
11
1
1.21E+03
2.92E+03
2.41
3.16E+03
8.01E-01
9.66E+01
DSO
12
0.631
7.60E+02
2.09E+03
2.75
3.52E+03
8.01E-01
6.80E+01
DSO
13
0.398
4.63E+02
1.46E+03
3.16
3.86E+03
8.01E-01
4.70E+01
DSO
14
0.251
2.79E+02
1.01E+03
3.63
4.18E+03
8.01E-01
3.21E+01
DSO
15
0.158
1.68E+02
6.88E+02
4.1
4.47E+03
8.01E-01
2.17E+01
DSO
16
0.1
1.01E+02
4.63E+02
4.59
4.73E+03
8.01E-01
1.45E+01
DSO
四：FS实验数据处理。